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研究了甲基苯基二氯硅烷与苯基三氯硅烷的共水解缩合反应,探讨了甲基苯基二氯硅烷含量、反应温度、水的用量及反应时间对水解缩聚反应的影响,确定了最佳工艺。采用红外、核磁等手段对水解缩聚产物进行了结构表征。
The hydrolysis and condensation reaction of methylphenyl dichlorosilane and phenyltrichlorosilane were studied. The effects of the content of methylphenyl dichlorosilane, the reaction temperature, the amount of water and the reaction time on the hydrolysis and polycondensation reaction were discussed. The best technology. The structure of hydrolyzed polycondensation product was characterized by IR, NMR and other means.