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目的:建立苏南山肚痛丸的质量标准。方法:采用TLC法鉴别陈皮、血竭、甘草、丹参;采用HPLC法测定芍药苷的含量。结果:薄层色谱中斑点清晰,易于观察;芍药苷线性范围是6.3～105μg·ml~(-1),r=0.9999,平均回收率为102.5%,RSD为0.4%(n=6)。结论:方法简便、专属、准确,可作为本品的质量控制。
Objective: To establish the quality standards for the Sunan Shanbeitong pills. Methods: TLC method was used to identify Citrus chinense, D. chinensis, Radix Glycyrrhizae and Radix Salviae miltiorrhiza. The content of Paeoniflorin was determined by HPLC. RESULTS: The spots in TLC were clear and easy to observe. The linear range of paeoniflorin was 6.3-105 μg·ml -1, r=0.9999, the average recovery was 102.5%, and the RSD was 0.4% (n=6). Conclusion: The method is simple, exclusive, accurate, and can be used as the quality control of this product.