【摘 要】
：
The title compound (C40H42N2) has been synthesized by the reaction of 1-(1-naphthyl)-1-phenyl-3-chloropropylene and bis(4-(diethylamino) phenyl)methanone, and c
【机 构】
：
Fine Chemicals Department
论文部分内容阅读
The title compound (C40H42N2) has been synthesized by the reaction of 1-(1-naphthyl)-1-phenyl-3-chloropropylene and bis(4-(diethylamino) phenyl)methanone, and characterized by IR, 1H NMR, MS and X-ray diffraction analysis. The crystal belongs to the monoclinic system, space group P21/c with a = 17.047(3), b = 10.807(2), c = 1&494(4) (A), β = 105.727(4)°, V=3279.4(11) A3, Mr = 550.76, Z = 4, Dc = 1.115 g/cm3, μ(MoKα) = 0.085 mm-1, F(000) = 1184, the final R = 0.0625 and wR = 0.1384 for 2276 observed reflections (I ＞ 2σ(Ⅰ)). X-ray analysis reveals that the butadiene fragment adopts a planar cisiod conformation and makes a dihedral angel of 69.4(2)° with the naphthalene ring.
其他文献
2-Phenoxy-4H-spiro { naphtho[2,3-e] [ 1 ,4,2]oxazaphosphinane-5,10-dione, 1 ′-cyclohexane}2-oxide (C22H20NO5P) was synthesized by the Mannich-type reaction of
Sixteen new 2-heterocyclomethyl-5-diphenylmethylenecyclopentanone hydrochlorides were designed and synthesized. The growth inhibitory effect of these compounds
The oxygenation constants and thermodynamic parameter (△H°, △S°) of a series of novel Co (Ⅱ) complexes with phenol ether bridged dihydroxamic acids CoL1-Co
A novel thermo-sensitive switching membrane has been prepared by radiation-induced simultaneous grafting N-isopropylacrylamide (NIPAAm) onto chitosan membrane.
It is proved that when solving Schr(o)dinger equations for radially symmetric potentials the effect of higher dimensions on the radial wave function is equivale
为探究吕家坨井田地质构造格局,根据钻孔勘探资料,采用分形理论和趋势面分析方法,研究了井田7
We propose an effective and useful numerical simulation scheme for the investigation of the ultra-fast laser pulses in tenuous plasmas. The accuracy of the meth
Luffaculin 1 purified from the seeds of Luffa acutangula belongs to the type 1 ribosome-inactivating proteins (RIPs). It has been crystallized by the vapor-diff
With the help of scattering-matrix method, the acoustic phonon ballistic transmission and the thermal conductivity are studied detailedly in a four-terminal str
New exact solutions expressed by the Jacobi elliptic functions are obtained to the long-short wave interaction equations by using the modified F-expansion metho