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The complex Fe(aapo)2Cl3 with chemical formula C14H16Cl3FeN4O4 was obtained by the reaction of FeCl3(6H2O with apo(HCl·apo = 2-amino pyridine N-oxide) in acetonitrile. The result shows that CH3CN has been hydrolysised with the water from FeCl3(6H2O d