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本文研究了高锰酸钾－抗坏血酸化学发光体系，建立了测定抗坏血酸的化学发光分析新方法。线性响应的浓度范围为５．０×１０￣（－７）ｍｏｌ／Ｌ～４．０×１０￣（－５）ｍｏｌ／Ｌ检出限为３．０×１０￣（－７）ｍｏｌ／Ｌ对２．５×１０￣（－６）ｍｏｌ／Ｌ抗坏血酸进行１０次平行测定，相对标准偏差为１．６％。考察了２２种物质的干扰情况。用于维生素Ｃ片剂及注射液中抗坏血酸含量测定，结果令人满意。
In this paper, potassium permanganate - ascorbic acid chemiluminescence system was established, and a new chemiluminescence method for the determination of ascorbic acid was established. The linear range was 5.0 × 10 -7 mol / L to 4.0 × 10 -5 mol / L and the detection limit was 3.0 × 10 -7 mol / L 10 parallel determinations of 2.5 × 10 -6 mol / L ascorbic acid showed a relative standard deviation of 1.6%. Investigated the interference of 22 substances. For vitamin C tablets and injection of ascorbic acid content determination, the results are satisfactory.