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目的］建立了ＧＣ—ＭＳ联用直接分析粘合剂中挥发性有机化合物。［方法］采用全扫描法分析了其组成，并用选择离子扫描及内标标准曲线法选择定量分析了粘合剂中１，２－二氯乙烷、苯、甲苯、乙苯、二甲苯。［结果］１，２－二氯乙烷浓度在 ０．００２～０．５０ｍｇ／ｇ，苯在 ０．００１～０．１８ｍｇ／ｇ，甲苯、乙苯在 ０．０１～０．６９ｍｇ／ｇ，二甲苯在 ０．０２～０. ６９ｍｇ／ｇ范围内呈现良好的线性关系，方法的最低检出浓度：１， ２－二氯乙烷为 ０.００２ｍｇ／ｇ，苯为 ０．００１ｍｇ／ｇ，甲苯、乙苯为０．０１ｍｇ／ｇ，二甲苯为０．０２ｍｇ／ｇ，变异系数为０．５％～５．７％。［结论］该方法准确快速。
OBJECTIVE] To establish a GC-MS for the direct analysis of volatile organic compounds in adhesives. [Method] The composition was analyzed by full scan method, and 1,2 - dichloroethane, benzene, toluene, ethylbenzene and xylene in the adhesive were quantitatively selected by selective ion scan and internal standard curve method. [Result] The concentration of 1,2-dichloroethane was 0.002-0.50 mg / g, the content of benzene was 0.001-0.18 mg / g, the concentration of toluene and ethylbenzene was 0.01-0.69 mg / g, Xylene in the range of 0.02 ~ 0. 69mg / g showed a good linear relationship, the minimum detectable concentration of the method: 1, 2-dichloroethane is 0.002mg / g, benzene is 0.001mg / g, Toluene, ethylbenzene 0.01mg / g, xylene 0.02mg / g, coefficient of variation of 0.5% to 5.7%. [Conclusion] The method is accurate and rapid.