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试验了水热分散和高能球磨分散两种在沸石分子筛ZSM- 5 中分散MoO3 的新方法,并以X 光衍射、红外、吸附、紫外漫反射测试手段进行了表征。对制备方法、原理、分散量、适用条件及可能出现的X 光衍射和红外光谱的特点,与已有的热扩散、微波辐照法进行了对比研究。
A new method of dispersing MoO3 in zeolitic molecular sieve ZSM-5 by hydrothermal dispersion and high-energy ball milling dispersion was tested. The X-ray diffraction, infrared, adsorption and UV diffuse reflectance measurements were used to characterize the new method. The preparation method, principle, dispersion, applicable conditions and possible characteristics of X-ray diffraction and infrared spectroscopy were compared with the existing thermal diffusion and microwave irradiation methods.