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在微波辐射条件下,由2,3,3-三甲基-3H-吲哚高氯酸盐、1-苯基-3-(4’-硝基苯基)-2-丙烯-1-酮与哌啶合成了标题化合物。在甲醇/乙醇=1/1(V/V)中培养出单晶,通过X射线单晶结构分析法测定了分子结构和晶体结构,晶体属于单斜晶系,P2(1)/n空间群,其晶胞参数为:a=1.2507(4)nm,b=1.4378(4)nm,c=1.3033(4)nm,V=2.3366(12)nm3,Dc=1.401g/cm3,μ=0.210mm-1,F(000)=1024,Z=4,R1=0.0553,wR2=0.0732。
Under microwave irradiation conditions, 2,3,3-trimethyl-3H-indole perchlorate, 1-phenyl-3- (4’-nitrophenyl) The title compound was synthesized with piperidine. Single crystals were grown in methanol / ethanol = 1/1 (V / V), and the molecular structure and crystal structure were determined by X-ray single crystal structure analysis. The crystals belong to the monoclinic space group P2 (1) / n (4) nm, c = 1.3033 (4) nm, V = 2.3366 (12) nm3, Dc = 1.401g / cm3 and μ = 0.210mm -1, F (000) = 1024, Z = 4, R1 = 0.0553, wR2 = 0.0732.