Synthesis,characterization,properties and crystal structure of heterometallic 1D coordination polyme

来源 :Science in China(Series B:Chemistry) | 被引量 : 0次 | 上传用户:bartech
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Copper-zinc heterometallic 1D chain coordination polymer has been synthesized and characterized by elemental analysis, and IR spectra etc. The crystal structure was determined by single-crystal X-ray diffraction analyses. The title complex is 1D chain coordination polymer with the chemical formula {[CuLZn·CuLZn(H2O)]·H2O}n, where H4L=N-(2-hydroxybenzamido)-N’-(3-carboxy- lsalicylidene)ethylenediamine. Its structural unit is comprosed of two tetranuclear cycles formed by two dissymmetrical tetranuclear units. These units polymerized each other to form 1D chain coordi- nation polymer. Copper-zinc heterometallic 1D chain coordination polymer has been synthesized and characterized by elemental analysis, and IR spectra etc. The crystal structure was determined by single-crystal X-ray analysis. The title complex is 1D chain coordination polymer with the chemical formula { [CuLZn · CuLZn (H2O)] · H2O} n, where H4L = N- (2-hydroxybenzamido) -N ’- (3-carboxy- lsalicylidene) ethylenediamine. Its structural unit is comprosed of two tetranuclear cycles formed by two dissymmetrical tetranuclear units. These units polymerized each other to form 1D chain coordi- nation polymer.
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