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The title compound [Zn(Him2Py)(N3)2]2 (Zn2C26H38N18O2, Mr=765.48) has been prepared and structurally characterized by X-ray diffraction methods. It crystallizes in monoclinic, space group P21/n with α=10.989(3), b=11.519(3), c=13.812(4)A, β=101.700(5)