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The complex dimethylgallium- [4-nitro-2- (N-benzo- 15-crown-5 ) - 1 -phenoxide ] (C23H31 N2O7Ga) has been synthesized by the method reported. The crystal X-ray diffraction analysis shows that the crystal belongs to the triclinic with space group P1, M = 517. 23 and the unit cell parameters: a = 1. 4501 (2), b = 1. 5090(2), c = 1. 3865 (6)nm, a = 105. 58(1 ), β = 117. 26(2), γ = 66. 812(8)°, V= 2. 464546nm3, Z =4, Dc = 1. 39g· cm-3, u = 11. 6cm-1, F(000) = 1080, R = 0. 051, Rw = 0. 064. The coordination number of Ga is four and the gallium atom is located in a distorted tetrahedron structure.
The complex dimethylgallium- [4-nitro-2- (N-benzo- 15-crown-5) - 1 -phenoxide] (C23H31N2O7Ga) has been synthesized by the method reported. The crystal X-ray diffraction analysis shows that the crystal belongs to the triclinic with space group P1, M = 517. 23 and the unit cell parameters a = 1. 4501 (2), b = 1. 5090 (2), c = 1. 3865 (6) nm, a = 39.8 cm 3, u = 11, 105. 58 (1), β = 117. 26 (2), γ = 66. 812 (8) °, V = 2. 464546 nm 3, Z = 4, Dc = 1.39 g · cm -3. The coordination number of Ga is four and the gallium atom is located in a distorted tetrahedron structure.